100 %     1 out of 1 reviewer(s) would follow this procedure again.
 
Chen
Graduate Student at UC Berkeley
( ****@berkeley.edu )
Level 5 Reviewer
Member since : 12/2015

46 Reviews
5 Helpful votes

Posted on :
09/06/2016 23:27

Yield of (isolated) product

ee (if applicable)

Reaction Set-up

Workup and Isolation

Availability of reagents

Would recommend this procedure?

Yes

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Glovebox manipulation
Purified solvents
Air-stable product
Moisture-stable product
Column chromatography
Commercial reactants/reagents
Commercial catalysts

The literature says "Removal of the volatiles gave a brown solid which was used for subsequent reactions without further purification". I nevertheless ran an pretty straightforward column and obtained a almost colorless solid.

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